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RUST KNOCK OUT®INDEPENDENT TESTING

United States Testing Company, Inc. -- Freeze-Thaw Resistance and pH Test


Chemical Services Division
1415 Park Avenue -- Hoboken, New Jersey 07030 -- 201-792-2400

REPORT 0F TEST

November 13, 1991

SUBJECT: Client supplied on pint of paint marked AH2377 on 10/29/91.

AUTHORIZATION: Client's telephone conversation.

PURPOSE: Determine freeze-thaw resistance and pH.

TEST DATES: 10/29/91 to 11/06/91.

PROCEDURE: pH was determined by glass electrode in accordance with ASTM E-70. Freeze-thaw cycles were run in accordance with ASTM D-2243.

RESULTS: Test Result
  pH 7.3
  Freeze-thaw, cycles pass 6*
  *At 7 cycles large viscosity increase was observed visually.

ES Laboratories -- Comparison of Treated and Untreated Areas by XRD

CUSTOMER: Advanced Protective Products DATE: 8/3/89
REPORT NO: ES#9283 INV. NO.: L-9283
REPORTED AS: Comparison of Treated and Untreated Areas by XRD PO NO. Heiss

Sample No. AH 2377: (Water Base Rust Converter Primer)

XRD:
"Rusted Area" "Painted Area"
alpha Iron (Fe) - Metal Substr. X X
alpha FeO (OH) X not det.
gamma FeO (OH) X not det.
Calcite (CaCo3) not det. X
Aragonite (CaCo3) not det. X
Kaolinite (Clay) not det. X
Magnesium Silicate Hydroxide not det. X
alpha Fe2O3 (Hematite) not det. X
Test Procedure: Hanawalt Search Method (X-ray Diffraction)
Reference: Joint Committee for Powder Diffraction Standards (Formerly ASTM File) in co-operation with the ASTM, ACA, National Association of Corrosion Engineers, The American Ceramic Society, The Mineralogical Society of America and Canada, The Clay Minerals Society, et. al.
1) JCPDS Search Manual, 1984, International Centre for Diffraction Data; 1601 Park Lane, Swarthmore, PA 19081

United States Testing Company -- Paint Flexibility Report of Test


Chemical Services Division
1415 Park Avenue -- Hoboken, New Jersey 07030 -- 201-792-2400

REPORT 0F TEST

October 30, 1989

SUBJECT: One paint submitted and identified by the client as: AH2377 (red)

AUTHORIZATION: Client's letter dated September 14, 1989

PURPOSE: To determine the flexibility of the paint.

PROCEDURE: In accordance with ASTM D-1737.

RESULTS: Pass 1/8" Mandrel without cracking.


United States Testing Company -- Freeze Thaw Resistance Report of Test


Chemical Services Division
1415 Park Avenue -- Hoboken, New Jersey 07030 -- 201-792-2400

REPORT 0F TEST

October 30, 1989

SUBJECT: One paint submitted and identified by the client as: AH2377 (red)

AUTHORIZATION: Client's letter dated September 14, 1989.

PURPOSE: To determine the freeze thaw resistance of the paint

PROCEDURE: In accordance: with ASTM D-1211 modified.

Freeze thaw resistance was determined by subjecting coated steel panels (5) to 15 cycles of 1 hour at -20oF, 1 hour at -5oF and 1/2 hour at room temperature 70-75oF.

RESULTS: No change after 15 cycles.


United States Testing Company -- Volatile Organic Content (VOC) Report of Test


Chemical Services Division
1415 Park Avenue -- Hoboken, New Jersey 07030 -- 201-792-2400

REPORT 0F TEST

October 30, 1989

SUBJECT: One paint submitted and identified by the client as: AH2377 (red)

AUTHORIZATION: Client's letter dated September 14, 1989.

PURPOSE: To determine the volatile organic content (VOC) of the paint.

PROCEDURE: In accordance with ASTM D-3960.

RESULTS:

Test Units ASTM Results
Volatile content % weight D-2369 54.75
Unit weight lb./gal D-1475 10.98
Water content % weight D-3792 55.4
VOC % weight D-3960 <0.5
VOC lb./gal D-3960 <0.5
 
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